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Usp. Khim., 2011, Volume 80, Issue 4, Pages 315–334 (Mi rcr49)  

This article is cited in 36 scientific papers (total in 36 papers)

X-Ray diffraction structure diagnostics of nanomaterials

E. M. Moroz

Boreskov Institute of Catalysis SB RAS, Novosibirsk

Abstract: The review concerns the development and applications of the X-ray diffraction method of the radial electron density distribution based on the integral analysis of X-ray diffraction in studies of nanomaterials, in particular, oxide supports for catalysts. The method provides information on the interatomic distances and coordination numbers in the structure and allows one to detect and estimate the size of nanostructures (phases) less than 3 nm in size, which cannot be detected by conventional powder X-ray diffraction analysis. The method is sensitive to the changes in the local structure measuring 1–3 unit cells; therefore, it is successfully used to identify various defects in nanoobjects of any chemical composition.

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English version:
Russian Chemical Reviews, 2011, 80:4, 293–312

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Document Type: Article
Received: 20.05.2010

Citation: E. M. Moroz, “X-Ray diffraction structure diagnostics of nanomaterials”, Usp. Khim., 80:4 (2011), 315–334; Russian Chem. Reviews, 80:4 (2011), 293–312

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    This publication is cited in the following articles:
    1. E. M. Moroz, “ChemInform Abstract: X-Ray Diffraction Structure Diagnostics of Nanomaterials”, ChemInform, 42:39 (2011), no  crossref
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    3. Tatyana Kardash, Ludmilla M. Plyasova, Dmitry I. Kochubey, Valentina M. Bondareva, Reinhard B. Neder, “Development of the local and average structure of a V–Mo–Nb oxide catalyst with Mo5O14-like structure during synthesis from nanostructured precursors”, Zeitschrift für Kristallographie, 2012, 1202170219  crossref  isi  scopus
    4. Moroz E.M., “X-Ray Diffraction Method of the Radial Electron Density Distribution. Structure of Nanophase Supports and Supported Catalysts”, J. Struct. Chem., 53:1 (2012), S63–S85  crossref  isi  scopus
    5. Plyasova L.M., Kardash T.Yu., “In Situ High-Temperature X-Ray Diffraction Measurements: Application to the Study of Heterogeneous Catalysts”, J. Struct. Chem., 53:1 (2012), S86–S108  crossref  isi  scopus
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    21. Xu T., Li M., “Size and Shape of Grain Boundary Network Components and Their Atomic Structures in Polycrystalline Nanoscale Materials”, J. Appl. Phys., 118:16 (2015), 164302  crossref  isi  scopus
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