M. I. Savchuk, A. P. Krinochkin, A. Rammohan, A. F. Khasanov, D. S. Kopchuk, I. N. Egorov, S. Santra, G. V. Zyryanov, V. L. Rusinov, O. N. Chupakhin, “An expedient synthesis of 5-alkynyl-6-aryl-2,2′-bipyridines”, Mendeleev Commun., 30:5 (2020), 610

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Mendeleev Communications, 2020, Volume 30, Issue 5, Pages 610–611
DOI: https://doi.org/10.1016/j.mencom.2020.09.019 (Mi mendc1268)

This article is cited in 7 scientific papers (total in 7 papers)

Communications

An expedient synthesis of 5-alkynyl-6-aryl-2,2′-bipyridines

M. I. Savchuk^a, A. P. Krinochkin^ab, A. Rammohan^a, A. F. Khasanov^ab, D. S. Kopchuk^ab, I. N. Egorov^a, S. Santra^a, G. V. Zyryanov^ab, V. L. Rusinov^ab, O. N. Chupakhin^ab

^a Institute of Chemical Engineering, Ural Federal University, Ekaterinburg, Russian Federation
^b I.Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences, Ekaterinburg, Russian Federation

Full-text PDF (159 kB) Citations (7) Supplementary materials

DOI: https://doi.org/10.1016/j.mencom.2020.09.019

Graphic abstract: An expedient synthesis of 5-alkynyl-6-aryl-2,2′-bipyridines

Abstract: 5-Alkynyl-6-aryl-2,2′-bipyridines were conveniently prepared in two steps comprising oxidative SN H ethynylation of 5-aryl-3-(2-pyridyl)-1,2,4-triazines at position 6. At the second step, the 1,2,4-triazine moiety was transformed into the pyridine one employing aza-Diels–Alder reaction with 2,5-norbornadiene.

Keywords: nucleophilic substitution of hydrogen, 1,2,4-triazines, acetylenes, 2,2′-bipyridines, aza-Diels–Alder reaction.

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Document Type: Article

Language: English

*Supplementary materials:*
		Supplementary_data_1.pdf	(2.4 Mb)

Citation: M. I. Savchuk, A. P. Krinochkin, A. Rammohan, A. F. Khasanov, D. S. Kopchuk, I. N. Egorov, S. Santra, G. V. Zyryanov, V. L. Rusinov, O. N. Chupakhin, “An expedient synthesis of 5-alkynyl-6-aryl-2,2′-bipyridines”, Mendeleev Commun., 30:5 (2020), 610–611

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https://www.mathnet.ru/eng/mendc1268

https://www.mathnet.ru/eng/mendc/v30/i5/p610

This publication is cited in the following 7 articles:

Citing articles in Google Scholar: Russian citations, English citations
Related articles in Google Scholar: Russian articles, English articles

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