A. V. Artem'ev, N. K. Gusarova, A. O. Korocheva, S. F. Malysheva, Yu. V. Gatilov, B. A. Trofimov, “A shortcut to tris[2-(4-hydroxyphenyl)ethyl]phosphine oxide and 2-(4-hydroxyphenyl)ethylphosphinic acid via reaction of elemental phosphorus with 4-tert-butoxystyrene”, Mendeleev Commun., 24:1 (2014), 29

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Mendeleev Communications, 2014, Volume 24, Issue 1, Pages 29–31
DOI: https://doi.org/10.1016/j.mencom.2013.12.009 (Mi mendc2462)

This article is cited in 6 scientific papers (total in 6 papers)

Communications

A shortcut to tris[2-(4-hydroxyphenyl)ethyl]phosphine oxide and 2-(4-hydroxyphenyl)ethylphosphinic acid via reaction of elemental phosphorus with 4-tert-butoxystyrene

A. V. Artem'ev^a, N. K. Gusarova^a, A. O. Korocheva^a, S. F. Malysheva^a, Yu. V. Gatilov^b, B. A. Trofimov^a

^a A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch of the Russian Academy of Sciences, Irkutsk, Russian Federation
^b N.N. Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch of the Russian Academy of Sciences, Novosibirsk, Russian Federation

Full-text PDF (340 kB) Citations (6)

DOI: https://doi.org/10.1016/j.mencom.2013.12.009

Graphic abstract: A shortcut to tris[2-(4-hydroxyphenyl)ethyl]phosphine oxide and 2-(4-hydroxyphenyl)ethylphosphinic acid <i>via</i> reaction of elemental phosphorus with 4-<i>tert</i>-butoxystyrene

Abstract: Red phosphorus reacts with 4-tert-butoxystyrene in KOH/DMSO system to afford (depending on the reaction conditions) tris(4-tert-but- oxyphenylethyl)phosphine oxide (48% yield) and/or 4-tert-butoxyphenylethylphosphinic acid (30% yield). The treatment of these products with aqueous HCl (45°C, 5min) quantitatively delivers tris[2-(4-hydroxyphenyl)ethyl]phosphine oxide and 2-(4-hydroxyphenyl)ethyl-phosphinic acid.

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Document Type: Article

Language: English

Citation: A. V. Artem'ev, N. K. Gusarova, A. O. Korocheva, S. F. Malysheva, Yu. V. Gatilov, B. A. Trofimov, “A shortcut to tris[2-(4-hydroxyphenyl)ethyl]phosphine oxide and 2-(4-hydroxyphenyl)ethylphosphinic acid via reaction of elemental phosphorus with 4-tert-butoxystyrene”, Mendeleev Commun., 24:1 (2014), 29–31

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https://www.mathnet.ru/eng/mendc/v24/i1/p29

This publication is cited in the following 6 articles:

Citing articles in Google Scholar: Russian citations, English citations
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