N. N. Yusifov, V. M. Ismayilov, N. D. Sadigova, M. N. Kopylovich, K. T. Mahmudov, “A straightforward synthesis of 2(3),6,6-trimethyl- 6,7-dihydrobenzofuran-4(5H)-ones”, Mendeleev Commun., 23:5 (2013), 292

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Mendeleev Communications, 2013, Volume 23, Issue 5, Pages 292–293
DOI: https://doi.org/10.1016/j.mencom.2013.09.019 (Mi mendc2694)

This article is cited in 6 scientific papers (total in 6 papers)

Communications

A straightforward synthesis of 2(3),6,6-trimethyl- 6,7-dihydrobenzofuran-4(5H)-ones

N. N. Yusifov^a, V. M. Ismayilov^a, N. D. Sadigova^a, M. N. Kopylovich^b, K. T. Mahmudov^ab

^a Department of Chemistry, Baku State University, Baku, Azerbaijan
^b Departimento de Engenharia Química, Instituto Superior Técnico, Universidade Técnica de Lisboa, Lisboa, Portugal

Full-text PDF (265 kB) Citations (6)

DOI: https://doi.org/10.1016/j.mencom.2013.09.019

Abstract: Alkylation of dimedone with 1,2,3-trichloro- or 1,2,3-tribromopropanes in the presence of K₂CO₃ in DMSO follows both O- and C-alkylation pathways giving 3-(2-haloprop-2-enyloxy)-5,5-dimethylcyclohex-2-enone and 2-(2-haloprop-2-enyl)-3-hydroxy-5,5-di- methylcyclohex-2-enone. These compounds on heating afford 3,6,6-trimethyl- and 2,6,6-trimethyl-6,7-dihydrobenzofuran-4(5H)-ones, respectively.

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Document Type: Article

Language: English

Citation: N. N. Yusifov, V. M. Ismayilov, N. D. Sadigova, M. N. Kopylovich, K. T. Mahmudov, “A straightforward synthesis of 2(3),6,6-trimethyl- 6,7-dihydrobenzofuran-4(5H)-ones”, Mendeleev Commun., 23:5 (2013), 292–293

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https://www.mathnet.ru/eng/mendc/v23/i5/p292

This publication is cited in the following 6 articles:

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