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This article is cited in 5 scientific papers (total in 5 papers)
Identification of the [1,3]dithiolo[4,5-d]dithiazolyl radical
S. A. Amelicheva, V. V. Popova, L. S. Konstantinovaa, S. P. Golovaa, V. V. Novikovb, E. D. Lubuzha, L. V. Mikhalchenkoa, V. P. Gul'tyaia, O. A. Rakitina
a N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation
b A.N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Moscow, Russian Federation
Abstract:
The synthesis of 5-oxo[1,3]dithiolo[4,5-d][1,3,2]dithiazol-1-ium chloride 1a from easily available zink chelate, TEA[Zn(DMIT)2], has been developed; salt 1a has been converted to the first representative of [1,3]dithiolo[4,5-d]dithiazolyl radical, which was identified by EPR and CV data.
Keywords:
1,3,2-dithiazolyl radicals, synthesis, 1,3,2-dithiazolium salts, reduction, cyclic voltammetry, EPR spectroscopy.
Citation:
S. A. Amelichev, V. V. Popov, L. S. Konstantinova, S. P. Golova, V. V. Novikov, E. D. Lubuzh, L. V. Mikhalchenko, V. P. Gul'tyai, O. A. Rakitin, “Identification of the [1,3]dithiolo[4,5-d]dithiazolyl radical”, Mendeleev Commun., 20:2 (2010), 80–82
Linking options:
https://www.mathnet.ru/eng/mendc2996 https://www.mathnet.ru/eng/mendc/v20/i2/p80
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