Abstract:
Crystal structure of widely employed precatalyst [Pd(Ph3P)4] is reported. It crystallizes in P-3 space group [a = 19.0828(8) and c = 26.4423(18) Å] with six molecules per unit cell. It is demonstrated that the phase purity of this important compound can now be routinely controlled via powder X-ray diffraction analysis.
Citation:
T. S. Sukhikh, M. P. Davydova, A. V. Artem’ev, “Crystal structure of tetrakis(triphenylphosphine)palladium(0)”, Mendeleev Commun., 33:2 (2023), 171–173
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https://www.mathnet.ru/eng/mendc340
https://www.mathnet.ru/eng/mendc/v33/i2/p171
This publication is cited in the following 4 articles: