R. G. Kostyanovsky, P. E. Dormov, P. T. Trapencieris, B. Strumfs, G. K. Kadorkina, I. I. Chervin, I. Ya. Kalvin's, “Optically active 2,2-dimethyl-1,3,4-triazabicyclo[4.1.0]heptan-5-one: synthesis, spontaneous resolution and absolute configuration”, Mendeleev Commun., 9:1 (1999), 26

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Mendeleev Communications, 1999, Volume 9, Issue 1, Pages 26–27
DOI: https://doi.org/10.1070/MC1999v009n01ABEH001047 (Mi mendc4511)

This article is cited in 11 scientific papers (total in 11 papers)

Optically active 2,2-dimethyl-1,3,4-triazabicyclo[4.1.0]heptan-5-one: synthesis, spontaneous resolution and absolute configuration

R. G. Kostyanovsky^a, P. E. Dormov^a, P. T. Trapencieris^b, B. Strumfs^b, G. K. Kadorkina^a, I. I. Chervin^a, I. Ya. Kalvin's^b

^a N.N. Semenov Federal Research Center for Chemical Physics, Russian Academy of Sciences, Moscow, Russian Federation
^b Latvian Institute of Organic Synthesis, Riga, Latvian Republic

Full-text PDF (88 kB) Citations (11)

DOI: https://doi.org/10.1070/MC1999v009n01ABEH001047

Abstract: Bicycle (±)-1 crystallises as a conglomerate (space group P2₁) and undergoes spontaneous resolution on crystallisation from chloroform or acetone (16–44% ee). The absolute configuration (S)-(−)-1 was determined by synthesis from (S)-Ser-OMe; mutarotation due to the partial conversion of 1 into the corresponding isopropylidene 4 was observed in MeOH solution.

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Document Type: Article

Language: English

Citation: R. G. Kostyanovsky, P. E. Dormov, P. T. Trapencieris, B. Strumfs, G. K. Kadorkina, I. I. Chervin, I. Ya. Kalvin's, “Optically active 2,2-dimethyl-1,3,4-triazabicyclo[4.1.0]heptan-5-one: synthesis, spontaneous resolution and absolute configuration”, Mendeleev Commun., 9:1 (1999), 26–27

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https://www.mathnet.ru/eng/mendc/v9/i1/p26

This publication is cited in the following 11 articles:

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