R. G. Kostyanovsky, K. A. Lyssenko, G. K. Kadorkina, O. V. Lebedev, A. N. Kravchenko, I. I. Chervin, V. R. Kostyanovsky, “Chiral glycouril, 2,6-diethyl-2,4,6,8-tetraazabicyclo[3.3.0]octane-3,7-dione: spontaneous resolution, reactivity and absolute configuration”, Mendeleev Commun., 8:6 (1998), 231

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Mendeleev Communications, 1998, Volume 8, Issue 6, Pages 231–233
DOI: https://doi.org/10.1070/MC1998v008n06ABEH001035 (Mi mendc4743)

This article is cited in 27 scientific papers (total in 27 papers)

Chiral glycouril, 2,6-diethyl-2,4,6,8-tetraazabicyclo[3.3.0]octane-3,7-dione: spontaneous resolution, reactivity and absolute configuration

R. G. Kostyanovsky^a, K. A. Lyssenko^b, G. K. Kadorkina^a, O. V. Lebedev^c, A. N. Kravchenko^c, I. I. Chervin^a, V. R. Kostyanovsky^a

^a N.N. Semenov Federal Research Center for Chemical Physics, Russian Academy of Sciences, Moscow, Russian Federation
^b A.N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Moscow, Russian Federation
^c N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation

Full-text PDF (186 kB) Citations (27)

DOI: https://doi.org/10.1070/MC1998v008n06ABEH001035

Abstract: The title glycouril 1 was spontaneously resolved into enantiomers by crystallisation from H₂O and sorting of conglomerate crystals, then N-chlorination and N-aminomethylation to give 2, 3 and 4, respectively, were studied. The absolute configuration 1R,5R-(+) was determined by an X-ray diffraction study of diastereomeric N,N-bis-aminomethyl derivative (−)-4.

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Document Type: Article

Language: English

Citation: R. G. Kostyanovsky, K. A. Lyssenko, G. K. Kadorkina, O. V. Lebedev, A. N. Kravchenko, I. I. Chervin, V. R. Kostyanovsky, “Chiral glycouril, 2,6-diethyl-2,4,6,8-tetraazabicyclo[3.3.0]octane-3,7-dione: spontaneous resolution, reactivity and absolute configuration”, Mendeleev Commun., 8:6 (1998), 231–233

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This publication is cited in the following 27 articles:

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