S. I. Gorbin, A. A. Bakibaev, D. A. Kurgachev, V. S. Malkov, K. Yu. Novolokov, G. O. Sysoev, “Synthesis of 1-[1-(diphenoxyphosphoryl)alkyl]-3,4,6-trimethylglycolurils”, Mendeleev Commun., 33:5 (2023), 638

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Mendeleev Communications, 2023, Volume 33, Issue 5, Pages 638–639
DOI: https://doi.org/10.1016/j.mencom.2023.09.015 (Mi mendc480)

This article is cited in 3 scientific papers (total in 3 papers)

Communications

Synthesis of 1-[1-(diphenoxyphosphoryl)alkyl]-3,4,6-trimethylglycolurils

S. I. Gorbin, A. A. Bakibaev, D. A. Kurgachev, V. S. Malkov, K. Yu. Novolokov, G. O. Sysoev

Department of Chemistry, National Research Tomsk State University, Tomsk, Russian Federation

Full-text PDF (176 kB) Citations (3) Supplementary materials

DOI: https://doi.org/10.1016/j.mencom.2023.09.015

Graphic abstract: Synthesis of 1-[1-(diphenoxyphosphoryl)alkyl]-3,4,6-trimethylglycolurils

Abstract: The reaction of 1,3,4-trimethylglycoluril, aliphatic aldehydes and triphenyl phosphite in the presence of methanesulfonic acid affords new phosphorus-containing derivatives of glycoluril. The thus formed diastereomers of 1-[1-(diphenoxy-phosphoryl)alkyl]-3,4,6-trimethylglycolurils were separated by reverse-phase HPLC

Keywords: 1,3,4-trimethylglycolurils, phosphonates, diastereomers, Birum-Oleksyszyn reaction, triphenyl phosphite, one-pot synthesis.

Bibliographic databases:

Document Type: Article

Language: English

*Supplementary materials:*
		Supplementary_data_1.pdf	(1.5 Mb)

Citation: S. I. Gorbin, A. A. Bakibaev, D. A. Kurgachev, V. S. Malkov, K. Yu. Novolokov, G. O. Sysoev, “Synthesis of 1-[1-(diphenoxyphosphoryl)alkyl]-3,4,6-trimethylglycolurils”, Mendeleev Commun., 33:5 (2023), 638–639

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https://www.mathnet.ru/eng/mendc480

https://www.mathnet.ru/eng/mendc/v33/i5/p638

This publication is cited in the following 3 articles:

Citing articles in Google Scholar: Russian citations, English citations
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