D. A. Tatarinov, E. A. Mikulenkova, I. A. Litvinov, V. F. Mironov, “Efficient one-pot synthesis of 2-(2-hydroxyaryl)-2,4,4-trimethylchromanes from 1-(2-hydroxyaryl)ethanones”, Mendeleev Commun., 33:6 (2023), 850

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Mendeleev Communications, 2023, Volume 33, Issue 6, Pages 850–852
DOI: https://doi.org/10.1016/j.mencom.2023.10.037 (Mi mendc546)

Communications

Efficient one-pot synthesis of 2-(2-hydroxyaryl)-2,4,4-trimethylchromanes from 1-(2-hydroxyaryl)ethanones

D. A. Tatarinov^ab, E. A. Mikulenkova^ab, I. A. Litvinov^a, V. F. Mironov^a

^a A.E. Arbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of the Russian Academy of Sciences, Kazan, Russian Federation
^b Alexander Butlerov Institute of Chemistry, Kazan Federal University, Kazan, Russian Federation

Full-text PDF (413 kB) Supplementary materials

DOI: https://doi.org/10.1016/j.mencom.2023.10.037

Graphic abstract: Efficient one-pot synthesis of 2-(2-hydroxyaryl)-2,4,4-trimethylchromanes from 1-(2-hydroxyaryl)ethanones

Abstract: A one-pot synthesis of 2-(2-hydroxyaryl)-2,4,4-trimethyl-chromanes in near quantitative yields is based on the reaction of 1-(2-hydroxyaryl)ethanones with methylmagnesium iodide followed by treatment with dilute sulfuric acid. The structure of 2-(2-hydroxyphenyl)-2,4,4-trimethylchromane is confirmed by X-ray diffraction.

Keywords: 2,4,4-trimethylchromanes, 1-(2-hydroxyaryl)ethanones, Grignard synthesis, [4 + 2]-cycloaddition, dehydration, crystal structure.

Bibliographic databases:

Document Type: Article

Language: English

*Supplementary materials:*
		Supplementary_data_1.pdf	(1.1 Mb)

Citation: D. A. Tatarinov, E. A. Mikulenkova, I. A. Litvinov, V. F. Mironov, “Efficient one-pot synthesis of 2-(2-hydroxyaryl)-2,4,4-trimethylchromanes from 1-(2-hydroxyaryl)ethanones”, Mendeleev Commun., 33:6 (2023), 850–852

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https://www.mathnet.ru/eng/mendc/v33/i6/p850

Citing articles in Google Scholar: Russian citations, English citations
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