M.-x. Xu, K.-M. Zhang, “Rongalite-promoted transition metal-free synthesis of S-aryl phosphorothioates”, Mendeleev Commun., 32:3 (2022), 390

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Mendeleev Communications, 2022, Volume 32, Issue 3, Pages 390–392
DOI: https://doi.org/10.1016/j.mencom.2022.05.033 (Mi mendc674)

This article is cited in 5 scientific papers (total in 5 papers)

Communications

Rongalite-promoted transition metal-free synthesis of S-aryl phosphorothioates

M.-x. Xu^a, K.-M. Zhang^ab

^a Jiangsu Police Institute, Nanjing, P.R. China
^b Nanjing Institute of Technology, Nanjing, P.R. China

Full-text PDF (197 kB) Citations (5) Supplementary materials

DOI: https://doi.org/10.1016/j.mencom.2022.05.033

Graphic abstract: Rongalite-promoted transition metal-free synthesis of <i>S</i>-aryl phosphorothioates

Abstract: The improved procedure for the synthesis of S-aryl phosphorothioates from dialkyl phosphites (H-phosphonates), aryl iodides and elemental sulfur deals with the application of rongalite (sodium hydroxy-methanesulfinate) as the radical promoter. The reactions proceeded smoothly to give S-aryl phosphorothioates in good yields.

Keywords: rongalite, phosphorothioates, arylation, radical process, aryl halides, sulfur.

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Document Type: Article

Language: English

*Supplementary materials:*
		Supplementary_data_1.pdf	(1.3 Mb)

Citation: M.-x. Xu, K.-M. Zhang, “Rongalite-promoted transition metal-free synthesis of S-aryl phosphorothioates”, Mendeleev Commun., 32:3 (2022), 390–392

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https://www.mathnet.ru/eng/mendc/v32/i3/p390

This publication is cited in the following 5 articles:

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