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Mendeleev Communications, 2022, Volume 32, Issue 5, Pages 697–699
DOI: https://doi.org/10.1016/j.mencom.2022.09.044 (Mi mendc772) 		 
This article is cited in 3 scientific papers (total in 3 papers)

Communications

Synthesis of nanocrystalline magnesium oxide by thermolysis of magnesium citrate

Yu. E. Sinelnikovaab, N. F. Uvarovab

a Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch of the Russian Academy of Sciences, Novosibirsk, Russian Federation
b Novosibirsk State Technical University, Novosibirsk, Russian Federation
Full-text PDF (560 kB) Citations (3)
DOI: https://doi.org/10.1016/j.mencom.2022.09.044
Abstract: Magnesium citrate, obtained by dissolving magnesium oxide in an aqueous solution of citric acid, turned out to be a decahydrate of the composition Mg3(C6H5O7)2·10H2O, which was established by the results of synchronous thermal analysis, X-ray diffraction and IR spectroscopy. It is shown that the thermal decomposition of this salt proceeds in three stages in the temperature ranges of 120–250, 250–370 and 370–550 °C to form nanocrystalline magnesium oxide with grain sizes from 7 to 23 nm.
Keywords: magnesium citrate, Mg3(C6H5O7)2·10H2O, thermolysis mechanism, X-ray amorphous products, nanocrystalline magnesium oxide.
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Document Type: Article
Language: English


Citation: Yu. E. Sinelnikova, N. F. Uvarov, “Synthesis of nanocrystalline magnesium oxide by thermolysis of magnesium citrate”, Mendeleev Commun., 32:5 (2022), 697–699
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