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Mendeleev Communications, 2022, Volume 32, Issue 6, Pages 798–800
DOI: https://doi.org/10.1016/j.mencom.2022.11.030 (Mi mendc803) 		 
This article is cited in 1 scientific paper (total in 1 paper)

Communications

N-(Chlorodimethylsilyl)methyl anilides: synthesis and structure

A. S. Soldatenko, I. V. Sterkhova, N. F. Lazareva

A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch of the Russian Academy of Sciences, Irkutsk, Russian Federation
Full-text PDF (281 kB) Citations (1) Supplementary materials
DOI: https://doi.org/10.1016/j.mencom.2022.11.030
Abstract: N-(Chlorodimethylsilyl)methyl anilides of formula RC(O)N(C6H4X)CH2SiMe2Cl (R = Me, Ph; X = H, Me, Cl) were obtained by the reaction of N-TMS-containing anilides with ClCH2Si(Hal)Me2 (Hal = F, Cl). The silicon atom in these compounds is pentacoordinate according to the results of NMR and X-ray diffraction analysis.
Keywords: N-(chlorodimethylsilyl)methyl anilides, N-TMS anilides, chloromethyl(dimethyl)halogenosilanes, silicon pentacoordinate, NMR, X-ray diffraction analysis, organosilicon compounds.
Bibliographic databases:
Document Type: Article
Language: English
Supplementary materials:
Supplementary_data_1.pdf (1.2 Mb)


Citation: A. S. Soldatenko, I. V. Sterkhova, N. F. Lazareva, “N-(Chlorodimethylsilyl)methyl anilides: synthesis and structure”, Mendeleev Commun., 32:6 (2022), 798–800
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