L. Wang, D. Wang, J. Tang, “An efficient solvent-free thiocyanation of indoles by grinding”, Mendeleev Commun., 35:3 (2025), 269

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Mendeleev Communications, 2025, Volume 35, Issue 3, Pages 269–270
DOI: https://doi.org/10.71267/mencom.7677 (Mi mendc6591)

Communications

An efficient solvent-free thiocyanation of indoles by grinding

L. Wang, D. Wang, J. Tang

School of Chemical and Pharmaceutical Engineering, Changzhou Vocational Institute of Engineering, 213164 Changzhou, P. R. China

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DOI: https://doi.org/10.71267/mencom.7677

Graphic abstract: An efficient solvent-free thiocyanation of indoles by grinding

Abstract: An efficient thiocyanation of indoles by grinding with ammonium thiocyanate and hypervalent iodine reagents under solvent-free conditions has been developed. The reaction proceeded rapidly to provide the target 3-thiocyanatoindoles in 75–86% yields.

Keywords: thiocyanation, grinding, solvent-free, indole, hypervalent iodine(III) reagent, ammonium thiocyanate.

Funding agency	Grant number
333
0
This project was financially supported by the ‘333’ High-level Talent Project of Jiangsu Province, and Academic Leader Research Fund of Changzhou Vocational Institute of Engineering

Received: 07.11.2024
Accepted: 06.12.2024

Published: 31.03.2025

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Document Type: Article

Language: English

*Supplementary materials:*
		Supplementary_data_1.pdf	(1.4 Mb)

Citation: L. Wang, D. Wang, J. Tang, “An efficient solvent-free thiocyanation of indoles by grinding”, Mendeleev Commun., 35:3 (2025), 269–270

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