E. G. Chupakhin, G. P. Kantin, D. V. Dar'in, M. Yu. Krasavin, “Convenient preparation of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones in array format”, Mendeleev Commun., 31:1 (2021), 36

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Mendeleev Communications, 2021, Volume 31, Issue 1, Pages 36–38
DOI: https://doi.org/10.1016/j.mencom.2021.01.010 (Mi mendc826)

This article is cited in 14 scientific papers (total in 14 papers)

Communications

Convenient preparation of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones in array format

E. G. Chupakhin^ab, G. P. Kantin^a, D. V. Dar'in^a, M. Yu. Krasavin^ab

^a Institute of Chemistry, St. Petersburg State University, St. Petersburg, Russian Federation
^b Immanuel Kant Baltic Federal University, Kaliningrad, Russian Federation

Full-text PDF (218 kB) Citations (14)

DOI: https://doi.org/10.1016/j.mencom.2021.01.010

Graphic abstract: Convenient preparation of (<i>E</i>)-3-arylidene-4-diazopyrrolidine-2,5-diones in array format

Abstract: A practically convenient synthesis of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones from N-substituted maleimides via the Wittig reaction and the Regitz diazo transfer has been developed. In all 26 cases studied, only one chromatographic purification was required with no need for aqueous workup, which makes this protocol amenable to producing the emerging class of diazo compounds in parallel format.

Keywords: privileged structures, maleimides, Wittig reaction, Michael acceptors, diazo transfer, diazo compounds, parallel synthesis.

Document Type: Article

Language: English

*Supplementary materials:*
		Supplementary_data_1.pdf	(3.7 Mb)

Citation: E. G. Chupakhin, G. P. Kantin, D. V. Dar'in, M. Yu. Krasavin, “Convenient preparation of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones in array format”, Mendeleev Commun., 31:1 (2021), 36–38

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https://www.mathnet.ru/eng/mendc826

https://www.mathnet.ru/eng/mendc/v31/i1/p36

This publication is cited in the following 14 articles:

Citing articles in Google Scholar: Russian citations, English citations
Related articles in Google Scholar: Russian articles, English articles

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